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Preparation and Characterization of CuO Nanoparticles by Novel Sol-Gel Technique

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Title Preparation and Characterization of CuO Nanoparticles by Novel Sol-Gel Technique
 
Creator Aparna, Y.
Rao, K. Venkateswara
Subbarao, P. Srinivasa
 
Subject CuO nanoparticles
Sol-gel method
Catalytic activity
 
Description Recent developments of nanosize materials of metal and metal oxide particles are intensively pursued because of their prominence in different fields of applications. Among all the transition metal oxides, CuO is a potential candidate for the application of magnetic storage devices, solar energy transfer, sensors, and super capacitors etc. Moreover CuO nanoparticles act as a good catalyst in some of the chemical reactions. CuO nanoparticles were prepared by novel sol-gel method. In this technique CuCl2.6H2O is added with acetic acid and heated to 100 °C with continuous stirring. To control the ph of the above solution, NaOH is added to the solution till ph reached desired value. The color of the solution changed from blue to black with precipitation. The black precipitation was washed 3 – 4 times with distilled water. Finally the solution was centrifuged and dried in air for one day. The CuO nanoparticles were characterized by studying their structure with X-ray diffraction and composition by energy dispersive X-ray analysis. The size of the nanoparticles is estimated by particle size analyzer and transmission electron microscopy. The optical studies were carried out with Uv-Vis spectrophotometer.
When you are citing the document, use the following link http://essuir.sumdu.edu.ua/handle/123456789/29602
 
Publisher Сумський державний університет
 
Date 2012-12-19T13:05:51Z
2012-12-19T13:05:51Z
2012
 
Type Article
 
Identifier Y. Aparna, K. Venkateswara Rao, P. Srinivasa Subbarao, J. Nano- Electron. Phys. 4 No 3, 03005 (2012)
http://essuir.sumdu.edu.ua/handle/123456789/29602
 
Language en