The Effect of Raw Materials Molar Ratio in Mechanochemical Synthesis of Amorphous Fe-B Alloy Nanoparticles
Electronic Archive of Sumy State University
Переглянути архів Інформація| Поле | Співвідношення | |
| Title |
The Effect of Raw Materials Molar Ratio in Mechanochemical Synthesis of Amorphous Fe-B Alloy Nanoparticles
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| Creator |
Shajari, S.
Sarraf-Mamoory, R. |
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| Subject |
Amorphous
Nanoparticles Fe-B alloys Mechanochemical NaBH4 Grinding |
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| Description |
In this study, amorphous iron-boron alloy nanoparticles successfully synthesized by mechanochemical method. The raw materials were ferrous sulfate heptahydrate (FeSO4.7H2O) as a source of iron and sodium borohydride (NaBH4) as a reducing agent. Powders grinding was performed with different NaBH4/FeSO4.7H2O molar ratio. The results revealed that high active and completely amorphous particles could be synthesized with the molar ratio of 4:1 for NaBH4:FeSO4 in 10 minutes of grinding time. Various characterizations, such as the chemical analysis, atomic absorption spectroscopy (AAS), fourier transform infrared spectroscopy (FT-IR), x-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM) have been performed. The XRD results confirmed the formation of the amorphous phase. Other results also indicate the formation of amorphous alloy nanoparticles with an average particle size below 50 nm and the composition was Fe-10 Wt percent B. |
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| Publisher |
Sumy State University
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| Date |
2014-05-23T10:03:20Z
2014-05-23T10:03:20Z 2012 |
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| Type |
Article
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| Identifier |
Shajari, S.
The Effect of Raw Materials Molar Ratio in Mechanochemical Synthesis of Amorphous Fe-B Alloy Nanoparticles [Текст] / S. Shajari, R. Sarraf-Mamoory
// Nanomaterials: Applications & Properties (NAP-2012) : 2-nd International conference, Alushta, the Crimea, September 17-22, 2012 / Edited by: A. Pogrebnjak. - Sumy : Sumy State University, 2012. - V. 1, No1. - 01PCN25
http://essuir.sumdu.edu.ua/handle/123456789/34897 |
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| Language |
en
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