Unlocking the Secrets Behind the Resin-Gel Synthesis for the Controlled Formation of Anatase and Rutile
Electronic Archive of Sumy State University
Переглянути архів Інформація| Поле | Співвідношення | |
| Title |
Unlocking the Secrets Behind the Resin-Gel Synthesis for the Controlled Formation of Anatase and Rutile
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| Creator |
Franklyn, P.J.
Narrandes, A. |
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| Subject |
Titania
Resin-Gel PEG XRD TEM Flame Synthesis |
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| Description |
Resin-gel synthesis has the ability to become a powerful technique for the synthesis of multi-phase nanoparticles. This study aimed to take further steps into investigating the mechanism of the resin-gel synthesis based on phase differentiation of titania, in the hope to describe optimal synthetic conditions for desired polymorph production with tailored particle size. Solvent, polymer chain length, heating rate and the use of citric acid has been varied previously. The results obtained suggested that the working theory of the resin-gel synthesis may be incorrect as there was significant phase differentiation based on the solvent used. This work explored the effects of the stoichiometric ratio of PEG to TiCl4 and the effect of heating rates to clarify the reaction mechanism. |
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| Publisher |
Sumy State University
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| Date |
2014-05-26T06:50:04Z
2014-05-26T06:50:04Z 2012 |
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| Type |
Article
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| Identifier |
Franklyn, P.J.
Unlocking the Secrets Behind the Resin-Gel Synthesis for the Controlled Formation of Anatase and Rutile [Текст] / P.J. Franklyn, A. Narrandes
// Nanomaterials: Applications & Properties (NAP-2012) : 2-nd International conference, Alushta, the Crimea, September 17-22, 2012 / Edited by: A. Pogrebnjak. - Sumy : Sumy State University, 2012. - V.1, No1. - 01PCN40
http://essuir.sumdu.edu.ua/handle/123456789/34944 |
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| Language |
en
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