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The Effect of Calcination Temperature in NiFe2O4 Nanoparticles Synthesis with Microvawe Combustion Method

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Title The Effect of Calcination Temperature in NiFe2O4 Nanoparticles Synthesis with Microvawe Combustion Method
 
Creator Karakas, K.Z.
Boncukcuoglu, R.
Karakas, I.H.
Yılmaz, M.T.
 
Subject Nanoparticles
Nickel ferrite
Microwave
Calcination
 
Description Magnetic ferrites are a group of technologically important magnetic materials. Synthesis of nanocrystalline spinel ferrite has been investigated intensively in recent years due to their potential applications in
high-density magnetic recording, microwave devices, and magnetic fluids In this study, NiFe2O4 nano particles were prepared with microvawe combustion methods. In experiments, samples obtained by microvawe
method were calcined at various temperatures. The structural and morphological properties of NiFe2O4
nano particles was determined by X-ray powder diffraction (XRD) and Scanning Electron microscopy
(SEM). Results showed that increasing calcination temperature contributed to cyristallinity of NiFe2O4
nanoparticles. But also average particle size increased. As a result, average particle size calculated by using Debye-Scherrer Formula as aproximately 30 nm. However, this results was confirmed with SEM
analysis.
 
Publisher Sumy State University
 
Date 2014-05-26T11:40:08Z
2014-05-26T11:40:08Z
2012
 
Type Article
 
Identifier The Effect of Calcination Temperature in NiFe2O4 Nanoparticles Synthesis with Microvawe Combustion Method [Текст] / K.Z. Karakas, R. Boncukcuoglu, I.H. Karakas, T.M. Yilmaz // Nanomaterials: Applications & Properties (NAP-2012) : 2-nd International conference, Alushta, the Crimea, September 17-22, 2012 / Edited by: A. Pogrebnjak. - Sumy : Sumy State University, 2012. - V.1, No1. - 01PCN45
http://essuir.sumdu.edu.ua/handle/123456789/35025
 
Language en