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Structure and Properties of Ceramics Based on ZrO2, Synthesis by Solvotermal Method

Electronic Archive of Sumy State University

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Title Structure and Properties of Ceramics Based on ZrO2, Synthesis by Solvotermal Method
 
Creator Ivanisenko, V.V.
Sirota, V.V.
 
Subject Solvotermal synthesis
Ceramic
Nanocrystalline
Zirconium dioxide
 
Description Nanosized powders ZrO2-NiO with a particle size of 10 – 20 nm were obtained by the method of solvotermal
synthesis. It is shown that the processes of formation of nanoparticles of c(t)-ZrO2 and m-ZrO2 at the
given parameters of solvotermal synthesis take place at different speeds. Ceramic material based on nanosized
powders of ZrO2 was obtained by the cold isostatic pressing and further sintering. The microstructure,
phase composition and strength properties of ceramics were determined by the scanning electron microscopy
(SEM), transmission electron microscopy (TEM) with diffraction, X-ray phase analysis. Mechanical
properties of ceramic were evaluated by the value of compressive strength. Compressive strength of the
experimental samples was at 700 MPa.
 
Publisher Sumy State University
 
Date 2014-05-27T07:11:38Z
2014-05-27T07:11:38Z
2012
 
Type Article
 
Identifier Ivanisenko, V. V. Structure and Properties of Ceramics Based on ZrO2, Synthesis by Solvotermal Method / V. V. Ivanisenko, V. V. Sirota // Nanomaterials: Applications & Properties (NAP-2012) : 2-nd International conference, Alushta, the Crimea, September 17-22, 2012 / Edited by: A. Pogrebnjak. - Sumy : Sumy State University, 2012. - V. 1, No3. - 03CNN11
http://essuir.sumdu.edu.ua/handle/123456789/35091
 
Language en