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Synthesis of Nanosized Oxides by Thermal Decomposition of Citrate Precursors

Electronic Archive of Sumy State University

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Title Synthesis of Nanosized Oxides by Thermal Decomposition of Citrate Precursors
 
Creator Romanova, I.V.
Farbun, I.I.
Kirillov, S.A.
 
Subject Citrate precursors
Nanoporous materials
 
Description The paper describes the citric acid aided synthesis of single and mixed nanosized oxides of transition
metals (Zn, Cu, Co, Ni, Mn, Ce). Thermal analysis is used for determining the composition of precursors
and intermediates formed in the process of their pyrolysis and for finding minimal temperatures of the
formation of oxide. All samples studied are found to be nanoporous materials with predominant
mesoporosity. The greatest surface area is obtained for samples with metal to citric acid ratio as 1 : 2.
Overviewing the results of porosity studies one can reach a conclusion regarding the optimal composition
of the precursors for obtaining each of target materials of the best quality.
 
Publisher Sumy State University
 
Date 2014-05-27T10:45:08Z
2014-05-27T10:45:08Z
2013
 
Type Article
 
Identifier Romanova, I.V. Synthesis of Nanosized Oxides by Thermal Decomposition of Citrate Precursors [Текст] / I.V. Romanova, I.I. Farbun, S.A. Kirillov // Nanomaterials: Applications & Properties (NAP-2013) : 3-rd International conference, Alushta, the Crimea, Ukraine, September 16-21, 2013 / Edited by: A. Pogrebnjak. - Sumy : Sumy State University, 2013. - V.2, No2. - 02PCN10
http://essuir.sumdu.edu.ua/handle/123456789/35132
 
Language en